Distillation, when the Operation is made in their full Strength: The
_Orleans_ Wines, and those of _Blois_ afford yet more; but the best
are those of the Territories of _Cogniac_ and of _Andaye_, which are
however in the Number of those the least drank in _France_. Whereas
those of _Burgundy_ and of _Champaign_, though of a very fine Flavour,
are improper, because they yield but very little in Distillation.
It must also be farther observed, that all the Wines for Distillation,
as those of _Spain_, the _Canaries_, of _Alicant_, of _Cyprus_, of St.
_Perés_, of _Toquet_, of _Grave_, of _Hungary_, and others of the same
kind, yield very little Brandy by Distillation; and consequently would
cost the Distiller considerably more than he could sell it for. What is
drawn from them is indeed very good, always retaining the saccharine
Quality, and rich Flavour of the Wine from whence it is drawn; but as
it grows old, this Flavour often grows aromatic, and is not agreeable
to all Palates.
Hence we see, that Brandies always differ, according as they are
extracted from different Species of Grapes. Nor would there be so
great a Similarity as there is between the different kinds of _French_
Brandies, were the strongest Wines used for this Purpose: But this
is rarely the Case, the weakest and lowest-flavoured Wines only are
distilled for their Spirit, or such as prove absolutely unfit for any
other Use.
A large Quantity of Brandies is distilled in _France_ during the
Time of the Vintage; for all those poor Grapes that prove unfit for
Wine, are usually first gathered, pressed, their Juice fermented,
and directly distilled. This rids their Hands of their poor Wines at
once, and leaves their Casks empty for the Reception of better. It is
a general Rule with them not to distil any Wine, that will fetch any
Price as Wine; for, in this State, the Profits upon them are vastly
greater than when reduced to Brandies. This large Stock of small Wines,
with which they are almost over-run in _France_, sufficiently accounts
for their making such vast Quantities of Brandy in _France_, more than
other Countries, which lie in warmer Climates, and are much better
adapted to the Production of Grapes.
Nor is this the only Fund of their Brandies; for all the Wine that
turns eager, is also condemned to the Still; and, in short, all that
they can neither export, nor consume at home, which amounts to a large
Quantity; since much of the Wine, laid in for their Family Provision,
is so poor, as not to keep during the Time in spending.
Hence many of our _English_ Spirits, with proper Management, are
convertible into Brandies, that shall hardly be distinguished from the
foreign in many Respects, provided this Operation be neatly performed.
And, in particular, how far a Cyder Spirit, and a Crab Spirit, may,
even from the first Extraction, be made to resemble the fine and thin
Brandies of _France_, we would recommend to those Distillers, whose
Skill and Curiosity prompts them to Undertakings condemned by those who
only work mechanically, and scorn to deviate from the beaten Tract,
tho’ they have the fairest Prospect of acquiring Profit to themselves,
and a lasting Emolument to their Country.
CHAP. XIX.
_Of the Distillation of Rum._
Rum differs from what we simply call Sugar Spirit, as it contains
more of the natural Flavour, or essential Oil of the Sugar Cane; a
great deal of raw Juice, and even Parts of the Cane itself being often
fermented in the Liquor, or Solution, of which the Rum is prepared.
Hence we see from whence Rum derives its Flavour; namely, from the Cane
itself. Some, indeed, are of Opinion, that the unctuous or oily Flavour
of the Rum proceeds from the large Quantity of Fat used in boiling
the Sugar. This Fat, indeed, if coarse, will give a stinking Flavour
to the Spirit in our Distillations of the Sugar Liquor, or Wash, from
our refining Sugar-houses; but this is nothing like the Flavour of the
Rum; which, as we have already observed, is the Effect of the natural
Flavour of the Cane.
Great Quantities of Rum are made at _Jamaica_, _Barbadoes_, _Antigua_,
and other Sugar Islands: The Method of making it is this:
When a sufficient Stock of the Materials is got together, they add
Water to them, and ferment them in the common Method, though the
Fermentation is always carried on very slowly at first; because at
the Beginning of the Season for making Rum in the Islands, they want
Yeast, or some other Ferment to make it work; but after this, they,
by Degrees, procure a sufficient Quantity of the Ferment, which
rises up as a Head to the Liquor in the Operation; and thus they are
able afterwards to ferment, and make their Rum with a great deal of
Expedition, and in very large Quantities.
When the Wash is fully fermented, or to a due Degree of Acidity, the
Distillation is carried on in the common Way, and the Spirit is made
up Proof; though sometimes it is reduced to a much greater Degree of
Strength, nearly approaching to that of Alcohol, or Spirit of Wine; and
it is then called double distilled Rum.
It would be easy to rectify the Spirit, and bring it to a much greater
Degree of Purity than we usually find it to be of; for it brings over
in the Distillation a large Quantity of the Oil; and this is often so
disagreeable, that the Rum must be suffered to lie by a long time to
mellow before it can be used; whereas, if well rectified, its Flavour
would be much less, and consequently much more agreeable to the Palate.
The best State to keep Rum, both for Exportation, and other Uses, is
doubtless that of Alcohol, or rectified Spirits. In this manner, it
would be contained in half the Bulk it usually is, and might be let
down to the common proof Strength with Water when necessary: For the
common Use of making Punch, it would likewise serve much better in the
State of Alcohol; as the Taste would be cleaner, and the Strength might
always be regulated to a much greater Degree of Exactness than in the
ordinary Way.
If the Business of rectifying Rum was more nicely managed, it seems a
very practicable Scheme to throw out so much of the Oil, as to reduce
it to the fine light State of a clear Spirit, but lightly impregnated
with the Oil; in this State it would nearly resemble Arrac, as is
easily proved by mixing a very small Quantity of it with a tasteless
Spirit; for it then bears a very near Resemblance to Arrac in Flavour.
CHAP. XX.
_Of Sugar-Spirit._
We mean by a Sugar-Spirit, that extracted from the Washings, Scumings,
Dross, and Waste of a Sugar-baker’s Refining-house.
These recrementitious, or drossy Parts of the Sugar are to be diluted
with Water, fermented in the same manner as Molosses or Wash, and then
distilled in the common Method. And if the Operation be carefully
performed, and the Spirit well rectified, it may be mixed with foreign
Brandies, and even Arrac in a large Proportion, to great Advantage; for
this Spirit will be found superior to that extracted from Treacle, and
consequently more proper for these Uses.
CHAP. XXI.
_Of Raisin-Spirits._
BY Raisin-Spirits, we understand, that extracted from Raisins, after a
proper Fermentation.
In order to extract this Spirit, the Raisins must be infused in a
proper Quantity of Water, and fermented in the manner described in the
Chapter on Fermentation. When the Fermentation is completed, the whole
is to be thrown into the Still, and the Spirit extracted by a strong
Fire.
The Reason why we here direct a strong Fire, is, because by that
Means a greater Quantity of the essential Oil will come over the Helm
with the Spirit, which will render it much fitter for the Distiller’s
Purpose; for this Spirit is generally used to mix with common Malt
Goods; and it is surprizing how far it will go in this Respect, ten
Gallons of it being often sufficient to give a determining Flavour, and
agreeable Vinosity to a whole Piece of Malt Spirits.
It is therefore well worth the Distiller’s while to endeavour at
improving the common Method of extracting Spirits from Raisins; and
perhaps the following Hint may merit Attention.
When the Fermentation is completed, and the Still charged with
fermented Liquor, as above directed, let the whole be drawn off
with as brisk a Fire as possible; but instead of the Cask or Can,
generally used by our _English_ Distillers for a Receiver, let a large
Glass, called by Chemists, a Separating-Glass, be placed under the
Nose of the Worm, and a common Receiver applied to the Spout of the
Separating-Glass; by this means the essential Oil will swim upon the
Top of the Spirit, or rather low Wine, in the Separating-Glass, and may
be easily preserved at the End of the Operation.
The Use of this limpid essential Oil is well known to Distillers; for
in this resides the whole Flavour, and consequently may be used to
the greatest Advantage in giving that distinguishing Taste, and true
Vinosity, to the common Malt-Spirits.
After the Oil is separated from the low Wine, the Liquor may be
rectified in _Balneum Mariæ_ into a pure and almost tasteless Spirit,
and therefore well adapted to make the finest compound Cordials, or to
imitate or mix with the finest _French_ Brandies, Arracs, &c.
In the same Manner a Spirit may be obtained from Cyder. But as its
particular Flavour is not so desirable as that obtained from Raisins,
it should be distilled in a more gentle Manner, and carefully rectified
in the Manner we shall shew in the Chapter on Rectification; by which
Means a very pure and almost insipid Spirit will be obtained, which
may be used to very great Advantage in imitating the best Brandies of
_France_, or in making the finest compound Waters or Cordials.
CHAP. XXII.
_Of Arracs._
What is properly meant by the Term Arracs, are Spirits extracted from
the fermented Juice of certain Trees common in the _East-Indies_,
particularly those of the Cocoa, or Palm-tree. The whole Process of
making Arrac, is performed in the following Manner.
In order to procure the vegetable Juice for this Operation, the Person
provides himself with a sufficient Number of small earthen Pots, with
Bellies and Necks, resembling our common glass Bottles; a Number of
these he fastens to his Girdle, or to a Belt across his Shoulders, and
climbs up the tall Trunk of the Cocoa tree: Having reached the Boughs
of the Tree, he cuts off with a Knife certain small Buds, or Buttons,
applying immediately to the Wound one of his Bottles, and fastens it
with a String to the Bough. In this Manner he proceeds till he has
fixed his whole Number of Bottles, which serve as Receivers to the
Juice distilling from the Wounds. This Operation is generally performed
in the Evening, a greater Quantity of Juice flowing from the Tree in
the Night than in the Day. The Bottles are next Morning taken off,
and the Liquor emptied with a proper Vessel, where it spontaneously
ferments. As soon as the Fermentation is completed, the Liquor is
thrown into the Still, and drawn down to a low Wine; but so very poor
and dilute, that they are obliged to rectify it in another Still,
to that weak kind of Proof Spirit, we generally see it; for though
it appears Bubble-Proof, it rarely contains more than a sixth, and
sometimes only an eighth of Alcohol, all the rest being no more than
an acidulated Water, which might be supplied from any common Spring.
Why Arrac appears Bubble-Proof, when in reality so far below what we
mean by Proof, is not so great a Mystery, as at first Sight it appears
to be; for this kind of Proof is entirely owing to a certain Tenacity
of the Parts of the Liquor, or to the particular Property of the Oil
incorporated in the Spirit; as we shall abundantly shew in a subsequent
Chapter.
From this Account of Arrac, it should seem no very difficult Matter to
imitate it here. And, perhaps, the whole Difficulty lies in procuring
a pure and insipid Spirit; for it is ridiculous to attempt it with our
common Malt-Spirit. With regard to the Flavour of the Arrac, it may be
effectually imitated by some essential Oils easily procurable.
Hence we see of what prodigious Advantage a pure and insipid Spirit
would be of to Distillers, and consequently the great Encouragement
there is to attempt the Discovery. Perhaps a Spirit of this kind may be
extracted from Sugar properly refined. The Hint is worth prosecuting;
and the Writer of this Essay, from repeated Experiments, is abundantly
convinced that the Thing is practicable. Had he entirely succeeded,
he would readily have communicated the Whole for the Benefit of his
Country; but is now obliged to defer, to some future Opportunity, the
Result of his Enquiries. In the mean Time, he would recommend the
Prosecution of this Hint to those Distillers, who endeavour to improve
their Art, and advance it nearer to Perfection.
Since Arrac is a Spirit extracted from the Juice of the Cocoa tree, it
might perhaps be worth enquiring how nearly it might be imitated by
fermenting and distilling the Juices of the Birch and Sycamore-trees.
We should by this Means obtain an _English_ Arrac; and, perhaps, a
Spirit equal in Flavour to that imported from _Batavia_.
When the Cask, in which the Arrac is imported happens to be decayed;
or the Liquor touches any Nails, or other Iron, it dissolves Part of
it, and at the same time extracts the resinous Parts of the Oak, by
which means the whole Liquor in the Cask acquires an inky Colour. In
order to whiten and clarify Arrac, which has contracted this Colour, a
large Quantity of new or skimmed Milk must be put into the Cask, and
the whole beat together, as Vintners do to whiten their brown Wines; by
this means the inky Colour will be absorbed by the Milk, and fall with
it to the Bottom, so that the greatest Part of the Arrac may be drawn
off fine; and the Remainder procured in the same Condition by being
filtrated through a conical Flannel Bag.
CHAP. XXIII.
_Of Rectification._
There are several Methods of performing this Operation; though some,
and indeed those in general practiced by our Distillers, hardly deserve
the Name; because, instead of rectifying, that is freeing the Spirit
from its essential Oil and Phlegm, they alter the natural Flavour of
the Spirit that comes over in the Operation.
The principal Business of Rectification is to separate the Spirit
from the essential Oil of the Ingredient, which is very apt to adhere
strongly to the Spirit. And in order to this, Care should be taken in
the first Distillation; that is, the Spirit, especially that from Malt,
should be drawn by a gentle Fire, by which means great Part of the
essential Oil will be kept from mixing with the Spirit; for Experience
has abundantly proved, that it is much easier to keep asunder, than to
separate them when once mixed.
But as it is almost impossible to draw low Wines without the Spirit
being in some Measure impregnated with the essential Oil, it is
absolutely necessary to be acquainted with some Methods of separating
the Spirit from the Oil, and also of freeing it from its Phlegm. The
best Methods of doing this to Perfection, are Re-distillation and
Percolation.
In order to rectify low Wines, they should be put into a tall Body or
Alembic, and gently distilled in _Balneum Mariæ_; by this means a
large Proportion, both of the Oil and Phlegm will remain in the Body.
But if the Spirit should be found, after this Operation, to contain
some of the essential Oil, it must be let down with fair Water, and
re-distilled in the same gentle Manner. And thus it may be brought
to any Degree of Purity; especially if in the working the Spirit be
suffered to fall into a proper Quantity of clear Water, and the Spirit
afterwards rectified to the Height proposed. The same Method should be
used in freeing Proof Spirit, or even Alcohol, from this Oil; namely,
by letting it down with clean Water to the Strength of low Wines,
and re-distilling it in _Balneum Mariæ_. But it must be remembered,
that it is much more difficult to cleanse Alcohol, or Proof-Spirit
than low Wines, because the Oil is more intimately mixed with the two
former than with the latter. This Oil may however be separated from
Proof-Spirit, &c. by the Method already proposed, especially if it be
previously filtrated through Paper, thick Flannel, Sand, Stone, _&c._
But this Method, though it effectually answers the Intention, is
generally rejected by our Distillers, because of the Slowness of the
Operation; and others substituted in its stead, though instead of
freeing the Spirit from the Oil, they only abolish the natural Flavour
of the Spirit, and make a more intimate Mixture between the Particles
of the Spirit, and those of the essential Oil.
It is impossible to enumerate all the Methods practised by Distillers,
as almost every one pretends to have a secret Nostrum for this Purpose.
The principal Methods in use for rectifying Malt-Spirits, are however
reducible to three, namely, by fixed alcaline Salts, by acid Spirits
mixed with alcaline Salts, and by saline Bodies, and flavouring
Additions.
The Method of rectifying by alcaline Salts is thus performed. To every
Piece of Proof Spirit, add fourteen Pounds of dry Salt of Tartar,
fixed Nitre, or calcined Tartar; lute on the Head, and distil, by a
gentle Heat, but be very careful to leave out the Faints. By this
Method a large Proportion of the fœtid Oil will be left in the Still;
and what comes over with the Spirit will be greatly attenuated. But
this Operation is generally performed in a very different manner; for,
instead of distilling the Spirit in a gentle and equable manner, the
Still is worked in its full Force; by which means the Oil, which should
have remained in the Still, is driven over, and intimately mixed with
the Spirit; and, consequently, the whole Operation frustrated, and the
Spirit rendered much harder to cleanse than it was before.
But even when the Operation is performed according to the Rules of
Art, it is far from being perfect; for it is well known, that Part
of the fixed Salts become volatile in the Operation, pass over the
Helm, and intimately mixes with the essential Oil still contained in
the Spirits: by this means the Oil becomes more perfectly united with
the Spirits, and consequently much harder to be separated by repeated
Distillations. Nor is this all, for the Still being worked in its full
Force, the bitter Oil of the Malt, formed into a kind of liquid Soap in
the Still, by means of the alcaline Salt, is brought over the Helm with
the Faints, and suffered to mix with the Spirit, whereby it is rendered
almost as nauseous and ill-tasted as before the Operation. Besides, if
this Operation were performed in its utmost Perfection, it would never
answer the Intention; for the alcaline Salt destroys the Vinosity of
the Spirit; and consequently deprives it of one of its most valuable
Properties. Our Distillers are well acquainted with this Defect in the
Operation, and endeavour to supply it by an Addition of Acids. This is
what we call the second Method by Alcalies and Acids.
The Operation of rectifying by the Method of fixed Alcalies and Acids
is the same as that above described; the Spirit is drawn over from
fixed Alcalies as before; but in order to mortify the Alcali in the
Spirit, and restore its Vinosity, a proper Quantity of some acid
Spirit is added. Various kinds of Acids are used on this Occasion; but
principally those of the mineral Kind, because of their Cheapness;
as Oil of Vitriol, Spirit of Nitre, Oil of Sulphur, and the like. We
would, however, caution a young Distiller from being too busy with
these corrosive Acids, the sulphurous Spirit of Vitriol, dulcified
Spirit of Nitre, or Mr. _Boyle_’s acid Spirit of Wine well rectified,
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