is easily separated from the Water, by the separating Glass, in
the following manner: Stop the Spout of the separating Glass with
a Cork, and then fill it with the Orange-flower-water; when it has
stood a small time the Oil will float on the Surface. Then pull
out the Cork, and let the Water run out at the Spout into another
Receiver placed for that Purpose. As the Water runs out at the Spout
of the Separating-glass, let it be supplied at the Mouth, that the
Separating-glass may be always full of Water, till the whole is in
this manner poured into it. Then by gently inclining the Glass, pour
out all the Water in it through the Spout, and the Oil will remain in
the Separating-glass, and may be poured into another Bottle, and kept
separate from the Water. The double Orange-flower water is odoriferous;
but the essential Oil much more so.
Orange-flower-water is not at present so much used as formerly; but as
it is a very odoriferous Water, I thought the Method of making it would
be not unacceptable to the young Distiller.
The essential Oil, or Quintessence of Orange-flowers will make a very
grateful Cordial, by mixing it with a clean proof Spirit: The Method of
mixing it is this:
Take some fine Loaf Sugar, and drop on it the Quantity of Oil you
intend to dissolve in the Spirit, and rub them well together in a Glass
Mortar, which is what the Chemists call making an Oleosaccharum. Put
this Oleosaccharum into the Spirit; mix them well together, and dulcify
it with Sugar to your Taste. If the Spirit be too strong, it may be
lowered with Water; but you must observe, that if you add Water enough
to bring the Spirit considerably below Proof, it will turn milky; and
in order to render it fine, you must filtrate it thro’ thick Flannel,
or thin Paper. Twenty Drops of the essential Oil will be sufficient for
a Pint of Spirit, and the same Proportion to a larger Quantity.
CHAP. VII.
_Of Rose-water._
The Damask Rose is the Species intended to be used in this Operation;
it is of a very fragrant Smell, and flowers in _June_ and _July_. The
Water may be made either by the hot Still, the cold Still, or the
_Balneum Mariæ_. If the hot Still be used, the Leaves picked from the
Stalks must be put into the Still with a sufficient Quantity of Water
to prevent an Empyreuma, and the Water drawn off by a gentle Fire.
The Receiver must be luted with a Bladder to the Nose of the Worm, to
prevent the finest and most volatile Parts from evaporating, which they
would otherwise do, to the great Prejudice of the Water.
If the cold Still be used, the Rose Leaves either with the Dew on them,
or sprinkled with Water, must be laid on the Iron Plate, and covered
with the conical Head. A gentle Fire must then be made under the Plate,
and a Receiver luted with a Bladder to the Nose of the Still. The Water
will gradually distil into the Receiver, and be strongly impregnated
with the odoriferous Parts of the Roses.
The same Method with regard to the _Balneum Mariæ_ must be used in the
Distillation of Roses as in that of Orange-flowers, and therefore need
not be repeated here. We shall therefore only observe, that Rose-water
drawn either by the cold Still, or the _Balneum Mariæ_, is much
preferable to that drawn by the hot Still.
The Essence, or essential Oil of Roses is looked upon as one of the
most valuable Perfumes in the World; but at the same Time the most
difficult to be procured in any Quantity. A small Quantity of it is
made in _Italy_, but it has always been thought impossible to procure
it here; and, therefore, a Method of acquiring this valuable Commodity
will not, I presume, be disagreeable to the Reader.
Take a Quantity of Damask Rose Leaves, put them into a proper Vessel,
with a sufficient Quantity of Water, adding some mineral Acid, as
Spirit of Salt, Vitriol, _&c._ In this Menstruum let the Roses be
digested for fifteen Days; after which put the Whole into an Alembic,
and draw off the Water with a pretty brisk Fire. But, instead of the
common Receiver, a Separating-Glass must be placed under the Nose of
the Worm, and a Receiver added to the Tube of the Separating-Glass.
By this Means all the Oil or Essence will float on the Surface of the
Water in the Separating-Glass, and may easily be separated from it,
when the Operation is finished.
CHAP. VIII.
_Of Cinnamon-water._
Cinnamon is a thin fine Bark, rolled up in a sort of little Pipes, from
the thickness of a Goose-quill, to that of a Man’s Thumb, and sometimes
more, and about two or three Feet long. Its Colour brownish, with a
Mixture of red. It is of an extremely aromatic Smell, and of an acrid
and pungent, but very agreeable Taste. It is the interior, or second
Bark of a Tree that grows plentifully in _Ceylon_. The People who
gather it take off the two Barks together, and immediately separating
the outer one, which is rough, and has very little Fragrancy, they lay
the other to dry in the Shade in an airy Place, where it rolls itself
up into the Form wherein we see it.
The greatest Cheats in the Sale of Cinnamon, are the selling such as
has already had its essential Oil distilled from it, and dried again,
and the imposing Cassia Lignea in its Place. The first of these is
discovered by the want of Pungency in the Cinnamon; the second by
this, that the Cassia, when held a little Time in the Mouth, becomes
mucilaginous, which the true Cinnamon never does, Cinnamon is a noble
Drug, endued, with many capital Virtues; it strengthens the Viscera,
assists Concoction, dispels Flatulencies, and is a pleasant Cardiac.
_Recipe for one Gallon of simple Cinnamon-Water._
Take a Pound of the best Cinnamon grosly powdered, digest for
twenty-four Hours, in two Gallons of Water; put the Whole into an
Alembic, and draw over one Gallon with a pretty brisk Fire.
The Oil of Cinnamon, in which the specific Virtue of the Drug consists,
is very ponderous, and therefore will not come over the Helm unless the
Fire be pretty brisk, especially with a simple Water. It will therefore
be in vain to attempt distilling simple Cinnamon-water by the _Balneum
Mariæ_.
CHAP. IX.
_Of Fennel-water._
Fennel-water is extracted from a Seed larger and more beautiful than
that produced by our common Fennel; it is called _Sweet Fennel seed_,
being of a fragrant Smell, and aromatic sweet Taste, and is cultivated
in _France_ and _Italy_. It is to be chosen new, large and fair; but
when damp or dusty to be rejected.
_Recipe for one Gallon of Fennel-water._
Take one Pound of Sweet Fennel-seeds, and two Gallons of Water; put
them into an Alembic, and draw off one Gallon with a gentle Fire.
CHAP. X.
_Of Pepper-mint-water._
Pepper-mint is a very celebrated Stomachic, and on that account greatly
used at present, and its Simple Water often called for.
_Recipe for a Gallon of Pepper-mint-water._
Take of the Leaves of dried Pepper-mint, one Pound and a half; Water
two Gallons and a half; put all into an Alembic, and draw off one
Gallon, with a gentle Fire.
The Water obtained from Pepper-mint by Distillation in _Balneum Mariæ_,
is more fragrant and more fully impregnated with the Virtues of the
Plant than that drawn by the Alembic. The same may be said with regard
to that extracted by the cold Still; when the cold Still is used the
Plant must be green, and if possible committed to the still with the
Morning Dew upon it.
CHAP. XI.
_Of Spear-mint-water._
Spear-mint is also like Pepper-mint a great Stomachic, and therefore
constantly used.
_Recipe for one Gallon of Spear-mint-water._
Take of the Leaves of dried Spear-mint one Pound and a half; Water two
Gallons and a half; draw off by a gentle Fire one Gallon.
This Water, like that drawn from Pepper-mint, will be more fragrant if
distilled in _Balneum Mariæ_, or the cold Still; but if the latter be
used, the same Caution must be observed of distilling the Plant green.
CHAP. XII.
_Of Baum-water._
Baum is a plant well known in our Gardens. It flowers in _July_, and is
of a fine cordial Flavour; but so weak, that it is soon dissipated and
lost; nor is it easy to dry it so as to preserve its natural Scent.
Baum-water, therefore should be drawn when the Plant is green; and in
order to procure the Water in full Perfection, it should be cohobated,
or returned several times upon fresh Parcels of the Plant; by this
means a Water may be procured from Baum extremely rich, and of
considerable Use as a Cordial.
If the _Balneum Mariæ_ be used, the Water is much better than that
drawn by an Alembic. The Water drawn from this Plant by the cold Still
will also be very fragrant, and highly impregnated with the Virtues of
the Plant.
CHAP. XIII.
_Of Penny-royal-water._
Penny-royal, a Plant very common in _England_, is very warm, and its
Parts very subtile and penetrating: It is one of the first Plants
in Esteem in the present Practice, as well as in former Ages, as an
Attenuant and Uterine. It is good in Flatulences and Suppressions of
Urine, and by many is greatly recommended in Dropsies, Jaundices, and
other chronic Distempers. It communicates its Virtues to Water in
Infusion, and its simple Water has, perhaps, more Virtue than any
other kept in the Shops. But as it is requisite in order to obtain a
Water fully impregnated with the Virtues of Baum, to cohobate it on
fresh Parcels of the Plant; the Water drawn from green Penny-royal, on
the contrary, generally contains so large a Portion of the essential
Oil, that it is necessary to separate what floats on the Surface of the
Water, by the Separating-glass.
_Recipe for one Gallon of Penny-royal-water._
Take of the dried Leaves of Penny-royal one Pound and a half, of Water
three Gallons; draw off one Gallon with a gentle Fire.
The Water drawn from green Penny-royal by the cold Still, is very
fragrant, and fully impregnated with the Virtues of the Plant.
CHAP. XIV.
_Of_ Jamaica-_Pepper-water_.
_Jamaica_-Pepper, or Pimento, is the Fruit of a tall Tree growing
in the mountainous Parts of _Jamaica_, where it is much cultivated,
because of the great Profit arising from the cured Fruit, sent in large
Quantities annually into _Europe_.
It is gathered, when green, and exposed to the Sun for many Days on
Cloths, and frequently shaked and turned, till thoroughly dry; great
Care is taken during the Time of drying to defend the Fruit from the
Morning and Evening Dews; when thoroughly dried it is sent over to us.
It is a very noble Aromatic, and deserves to be used more frequently
than it is at present. The simple Water drawn from it is a better
Carminative than any other simple Water at present in use.
_Recipe for a Gallon of_ Jamaica-_Pepper-water_.
Take of _Jamaica_-Pepper half a Pound. Water two Gallons and a half;
draw off one Gallon, with a pretty brisk Fire. The Oil of this Fruit is
very ponderous, and therefore this Water is best made in an Alembic.
CHAP. XV.
_Of Castor-water._
This Drug is brought to us in the Pods or Bags that naturally contained
it, and these so much resemble the Testicles of an Animal, both in
their dry State, and when on the Body of the Creatures, that it is
no wonder People who did not examine their Situation on the Animal,
really took them for such; it is, however, a peculiar secreted Matter,
contained in Bags destined to receive it.
Castor is an indurated Substance, formed of a Matter once fluid; the
thinner Part of which has been evaporated by drying. It is a light and
friable Matter, of a moderately lax Texture, and of a deep dusky brown
Colour. It is of a somewhat acrid and bitterish Taste, and of a strong
fœtid Smell, which, to many, is very disagreeable.
The Animal that produces the Castor is by all Authors called Castor and
Fiber, and by the Vulgar, the Beaver.
The Castor of several Parts of the World differs in Goodness, and in
regard to the Care taken in the drying. The _Russian_ Castor has long
been the most esteemed, and the _New England_ kind the least.
Castor-water is of great Use in hysteric Cases, and all Diseases of the
Nerves; in Epilepsies, Palsies, and all Complaints of that kind.
_Recipe for making one Gallon of Castor-water._
Take of _Russia_ Castor an Ounce, of Water three Gallons; draw off one
Gallon with a pretty brisk Fire.
CHAP. XVI.
_Of Orange-peel-water._
The Orange is a Fruit too well known to need a Description here. The
Water is very grateful to the Taste, and often used in Fevers, &c.
_Recipe for one Gallon of Orange-peel-water._
Take of the outward yellow Rind of _Seville_ Oranges, four Ounces;
Water three Gallons and a half; draw off one Gallon by the Alembic,
with a pretty brisk Fire.
CHAP. XVII.
_Of the Water of Dill-seed._
Dill greatly resembles Fennel both in Root, Stalk, or Leaf, but rarely
grows so tall, or is so much branched; it bears the same kind of yellow
Umbels of Flowers, after which come Seeds rounder, broader, and
flatter than those of Fennel. The whole Plant is of a strong Scent,
less pleasant than Fennel. It grows in Gardens, and flowers and seeds
in _July_ and _August_. The Water drawn from the Seeds is heating and
carminative, good in Cholics, and all Disorders arising from Wind.
_Recipe for making a Gallon of the Water of Dill-seed._
Take of Dill-seed one Pound, Water three Gallons; distil off by the
Alembic one Gallon, with a pretty brisk Fire.
The Waters we have enumerated in this Part are those now commonly in
use; though there are many other Herbs, from whence Waters of great
Use may be drawn; but as the Method of Distillation is the same in
all, it would be of no Use to extend these Instructions to a greater
length; we shall therefore only observe, that when unfavourable Seasons
have prevented the Herbs from attaining a proper Degree of Perfection,
it will be necessary to increase their Proportion in extracting the
several Waters ordered to be drawn by the Alembic.
A
Complete System
OF
DISTILLATION.
PART III.
_Of making compound Waters and Cordials._
The Perfection of this grand Branch of Distillery depends upon the
Observation of the following general Rules, easy to be observed and
practised.
1. The Artist must always be careful to use a well cleansed Spirit, or
one freed from its own essential Oil, as were before observed, Part
I. Chap. xxiii. For as a compound Water is nothing more than a Spirit
impregnated with the essential Oil of the Ingredients, it is necessary
that the Spirit should have deposited its own.
2. Let the Time of previous Digestion be proportioned to the Tenacity
of the Ingredients, or the Ponderosity of their Oil. Thus Cloves and
Cinnamon require a longer Digestion before they are distilled than
Calamus Aromaticus or Orange-peel. Sometimes Cohobation (explained in
Part II. Chap. iii.) is necessary; for Instance, in making the strong
Cinnamon-water; because the essential Oil of Cinnamon is so extremely
ponderous, that it is difficult to bring it over the Helm with the
Spirit without Cohobation.
3. Let the Strength of the Fire be proportioned to the Ponderosity of
the Oil intended to be raised with the Spirit. Thus, for Instance, the
strong Cinnamon Water requires a much greater Degree of Fire than that
from lax Vegetables, as Mint, Baum, _&c._
4. Let only a due Proportion of the finest Parts of the essential Oil
be united with the Spirit; the grosser and less fragrant Parts of the
Oil not giving the Spirit so agreeable a Flavour, and at the same Time
renders it thick and unsightly. This may in a great Measure be effected
by leaving out the Faints, and making up to Proof with fine soft Water
in their stead.
These four Rules carefully observed will render this extensive Part of
Distillation far more perfect than it is at present. Nor will there
be any Occasion for the use of burnt Allum, White of Eggs, Isinglass,
_&c._ to fine down Cordial Waters; for they will presently be fine,
sweet and pleasant tasted, without any farther Trouble.
CHAP. I.
_Of strong Cinnamon Water._
We have already (Chap. viii. Part II.) described this Drug, and given
some Directions for chusing the best Sort, to which the Reader is
referred.
_Recipe for sixteen Gallons of strong Cinnamon Water._
Take eight Pounds of fine Cinnamon bruised, seventeen Gallons of clean
rectified Spirit, and two Gallons of Water. Put them into your Still,
and digest them twenty-four Hours with a gentle Heat; after which draw
off sixteen Gallons by a pretty strong Heat.
I have ordered a much larger Quantity of Cinnamon than is common among
Distillers, because when made in the Manner above directed, it is
justly looked upon as one of the noblest Cordial Waters of the Shops;
but when made in the common Way of two Pounds to twenty Gallons of
Spirit, as some have ordered, is only an Imposition on the Buyer. Some
also, to render the Goods cheaper, use equal Quantics of Cinnamon and
Cassia Lignea; but by this means the Cordial is rendered much worse;
and, therefore, if you desire a fine Cinnamon-water the above Recipe
will answer your Intention: But if a cheaper Sort be desired you may
lessen the Quantity of Cinnamon, and add Cassia Lignea in its stead.
If you would dulcify your Cinnamon-water, take double refined Sugar,
what Quantity you please, the general Proportion is, about two Pounds
to a Gallon, and dissolve it in the Spirit after you have made it up
Proof with clean Water. One general Caution is here necessary to be
added; namely, that near the End of the Operation you carefully watch
the Spirit as it runs into the Receiver, in order to prevent the Faints
mixing with the Goods. This you may discover by often catching some of
it, as it runs from the Worm in a Glass, and observing whether it is
fine and transparent; for as soon as ever the Faints begin to rise,
the Spirit will have an azure or bluish Cast. As soon therefore as you
perceive this Alteration, change the Receiver immediately; for if you
suffer the Faints to mix with your other Goods, the Value of the whole
will be greatly lessened. With regard to the Faints, they are to be
kept by themselves, and poured into the Still when a fresh Parcel of
the same Goods is to be made.
It is also necessary to observe here, once for all, that the Distillers
call all Goods made up Proof, _double Goods_; and those which are below
Proof, _single_. This Observation will be alone sufficient to instruct
the young Distiller, how he may at any Time turn his Proof or double
Goods into single.
CHAP. II.
_Of Clove Water._
Cloves, from whence this Water takes its Name, are the Fruit of a Tree
growing in the _Molucca_ Islands. The Figure of this Fruit is oblong,
and not very thick, resembling in some measure, a Nail. The Surface of
it is rough, and the Colour a dusky brown with an admixture of reddish.
The whole Fruit is of an extremely fragrant Smell, and of an acrid,
pungent, and very aromatic Taste. Cloves are to be chosen the largest,
fairest, darkest coloured, the heaviest and most unctuous on the
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